synthesis and crystal structures of new 5,5-azotetrazolates合成和晶体结构的新5、5 -azotetrazolates.pdf
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Crystals 2012, 2, 127-136; doi:10.3390/cryst2010 127
OPEN ACCESS
crystals
ISSN 2073-4352
/journal/crystals
Article
Synthesis and Crystal Structures of New 5,5-Azotetrazolates
1 2 1 1 3
Gerhard Laus , Volker Kahlenberg , Klaus Wurst , Herwig Schottenberger , Niko Fischer ,
Jörg Stierstorfer 3 and Thomas M. Klapötke 3,*
1 Faculty of Chemistry and Pharmacy, University of Innsbruck, 6020 Innsbruck, Austria;
E-Mails: gerhard.laus@uibk.ac.at (G.L.); klaus.wurst@uibk.ac.at (K.W.);
herwig.schottenberger@uibk.ac.at (H.S.)
2 Institute of Mineralogy and Petrography, University of Innsbruck, 6020 Innsbruck, Austria;
E-Mail: volker.kahlenberg@uibk.ac.at (V.K.)
3 Department of Chemistry, University of Munich (LMU), 81377 Munich, Germany;
E-Mails: finch@cup.uni-muenchen.de (N.F.); jstch@cup.uni -muenchen.de (J.S.)
* Author to whom correspondence should be addressed; E-Mail: tmk@cup.uni-muenchen.de;
Tel.: +49-89-2180-77491; Fax: +49-89-2180-77492 (T.M.K.).
Received: 27 December 2011; in revised form: 21 February 2012 / Accepted: 29 February 2012 /
Published: 15 March 2012
Abstract: Five new 5,5-azotetrazolate salts (amminsilver, trimethylsulfonium,
tetramethyl-phosphonium, trimethylsulfoxonium, 2-(hydroxyethyl)trimethylammonium)
were prepared and characterized. The crystal structures were determined by X-ray
diffraction. Interactions between the ions are identified and
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