脉冲程序溶剂抑制solvent4.pdf

PulseProgramCatalogue

NMRGuide4.0

Classical:

1Dwaterpresaturation:

Conventional(zgpr/zg0pr|ZGPR)

Usingcompositepulses(zgcppr|ZGCPPR)

Usingspoilgradient(zggppr)

Usingcompositepulseandspoilgradient(zgcpgppr)

Fromf2channel(zgf2pr/zg0f2pr)

Usingshapedpulseforoff-resonancepresaturation(zgps)

Jumpandreturn:

1-1scheme(p11)

1-3-3-1scheme(p1331)

Gradient-based:

1DWATERGATE:

Using3-9-19scheme(p3919gp|P3919GP)

Using90water-selectivepulses(zggpwg|ZGGPWG)

1DExcitationSculpting:

Using180water-selectivepulses(zgesgp)

UsingW5pulsetrain(zggpw5)

1DWETscheme:

Conventional(wet)

WithC-13decouplingonf2duringWETandAQ(wetdc|LC1DWTDC)

WithC-13decouplingonf2duringWET(wetdw)

RelatedExperiments:

oAllthese1DexperimentscanbeincorporatedinanymultidimensionalNMR

experiment.Pleaserefertoeachchaptertocheckthedifferentpossibilitiesfor2Dand

3Dsolvent-suppressedexperiments

oLC-NMRExperiments

zgcppr

zgpr

zggpw5

zggpwg

p3919gp

109876543210ppm